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KitAlysis High-Throughput Miyaura Borylation Reaction Screening Kit-Pack of 2



Related Categories Buchwald Ligands and Complexes, Catalysis and Inorganic Chemistry, Chemical Synthesis, Cross-Coupling, KitAlysis,
reaction suitability   reaction type: Buchwald-Hartwig Cross Coupling Reaction
  reaction type: Cross Couplings
  reaction type: Heck Reaction
  reaction type: Hiyama Coupling
  reaction type: Negishi Coupling
  reaction type: Sonogashira Coupling
  reaction type: Stille Coupling
  reaction type: Suzuki-Miyaura Coupling
  reagent type: catalyst
core: palladium
functional group   phosphine



Screening kit for Miyaura borylation reaction. Step-by-step user guides and a downloadable experimental excel sheets are provided in the below hyperlinks.
Step-by-Step Guide for Miyaura Borylation Reaction Screening Kit
Downloadable Experiment excel sheets

Each kit contains 2 customizable screening sets that include the following components:
• 6 x 4 pre-weighed catalysts in glass vials loaded with stir bars and topped with cap mat.
• 4 x 4 mL reaction vials with pre-weighed KOAc
• Bis(pinacolato)diboron (473294), tetrahydroxydiboron (754242), and pinacol (221171)
• 1 (2 mL) ampule each of toluene, THF, n-butanol, DMA, MeOH, MeCN, ethylene glycol and DIPEA.
• 1 NEW KitAlysis 24-Well Reaction Block Replacement Film.
• 4 stir bars for substrate stock solution vials.
• 1 internal standard.

Best when used with KitAlysis Benchtop Inertion Box and 24-well Reaction Block (sold separately).

Features and Benefits

• Designed and tested by synthetic chemists.
• Easily run 24-microscale reactions in parallel.
• 10 μmol reactions with 1 μmol catalyst, 3 equiv. base, 0.1 M concentration.
• Customizable Excel Template for quick calculations and easy incorporation into electronic laboratory notebooks.

Legal Information

KitAlysis is a trademark of Sigma-Aldrich Co. LLC

Kit component also available separately


Product #

Add to Cart

P(Cy3) Pd G3, 97% SDS 764175
Potassium acetate, anhydrous, free-flowing, Redi-Dri, ACS reagent, ≥99.0% SDS 791733
XPhos Pd G4, 95% SDS 804274
SPhos Pd G4 SDS 804282
RuPhos Pd G4 SDS 804290
DTBPF-Pd-G3 SDS 804975
cataCXium Pd G4 SDS 900349
Toluene, anhydrous, ZerO2®, 99.8% SDS 900522
Ethylene glycol, anhydrous, ZerO2®, 99.8% SDS 900631
N,N-Dimethylacetamide, anhydrous, ZerO2®, 99.8% SDS 900634
Tetrahydrofuran, anhydrous, inhibitor-free, ZerO2®, ≥99.9% SDS 900636
1-Butanol, anhydrous, ZerO2®, 99.8% SDS 900639
Methanol, anhydrous, ZerO2®, 99.8% SDS 900641
Acetonitrile, anhydrous, ZerO2®, 99.8% SDS 900644
N,N-Diisopropylethylamine, purified by redistillation, ZerO2®, 99.5% SDS 900690
Pinacol, 98% SDS 221171
Bis(pinacolato)diboron, 99% SDS 473294
Tetrahydroxydiboron, 95% SDS 754242
Biphenyl, ReagentPlus®, 99.5% SDS B34656
Spinbar® magnetic stirring fleas, red, L 10 mm, diam. 3 mm SDS Z118850
KitAlysis 24-well reaction block replacement film SDS Z742110
Safety & Documentation

Safety Information

UN 3316 9


Certificate of Analysis (COA)

Please Enter a Lot Number
Protocols & Articles


KitAlysis™ 24-Well Reaction Block and Screwdriver Set

KitAlysis™ 24-Well Reaction Block KitAlysis™ Torque Screwdriver set KitAlysis™ Reaction Block Replacement Screws (10)
Keywords: Coupling reactions, Cross couplings

KitAlysis™ Benchtop Inertion Box

The Aldrich® KitAlysis™ Benchtop Inertion Box provides an inert environment to run oxygen sensitive cross-coupling reactions easily and robustly in a laboratory fume hood.
Keywords: Coupling reactions, Cross couplings

KitAlysis™ High-Throughput Screening Platform

In the high-pressure environment of discovery chemistry, time is everything. While general catalytic methods exist, substrate dependency makes it difficult to predict optimal conditions in practice. ...
Keywords: Catalysis, Chemical reactions, Solvents


Protocol KitAlysis™ High-Throughput Miyaura Borylation Reaction Screening Kit

2 bases (KOAc, DIEA) 6 degassed solvents (toluene, DMA, THF, n-butanol, MeOH, MeCN) 6 pre-weighed catalysts (x4)
Keywords: Addition reactions, Derivatizations, High performance liquid chromatography, Miyaura Borylation Reaction, PAGE, Solvents, Thin layer chromatography

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